仪器科学与技术

单晶硅多晶面表面波波速曲线超声测量方法

展开
  • 北京工业大学机械工程与应用电子技术学院 北京 100124

收稿日期: 2017-03-04

  修回日期: 2017-08-25

  网络出版日期: 2018-03-20

基金资助

国家自然科学基金资助项目(51575015,11172014,51505013)。

Measurement of Surface Acoustic Wave Velocity Curves of Silicon Crystal by Ultrasonic Method

Expand
  • College of Mechanical Engineering and Applied Electronic Technology, Beijing University of Technology, Beijing 100124

Received date: 2017-03-04

  Revised date: 2017-08-25

  Online published: 2018-03-20

摘要

随着晶体材料在航空航天、交通、电子电气工程、能源和环保等领域的广泛应用,对材料特殊性能的研究和检测工作也提出了新的要求。基于声波在材料中传播特性与材料力学性能之间的本构关系,建立单晶硅弹性常数矩阵与表面波波速之间关系的声弹性理论模型,并利用晶面的转换矩阵得到不同晶面下,表面波波速随角度变化的理论曲线。基于线聚焦超声换能器、高精度散焦测量系统和Vf,z)分析法获得单晶硅三个晶面沿不同角度的表面波波速变化曲线,试验测量结果与理论曲线相吻合,表明超声显微镜技术在各向异性材料表面波波速测量方面具有很高的精确度和可靠性。同时,论文还研究了单晶硅的晶体结构与表面波波速之间内在对应关系,为单晶硅等各向异性材料的性能检测与评价奠定了理论与试验基础。

本文引用格式

宋国荣, 洪广富, 卢东, 吕炎, 何存富, 吴斌 . 单晶硅多晶面表面波波速曲线超声测量方法[J]. 机械工程学报, 2018 , 54(6) : 110 -117 . DOI: 10.3901/JME.2018.06.110

Abstract

As the crystal materials are applied widely in the fields of aerospace, transportation, electrical and electronic engineering, energy and environmental protection, the new requirements for the researches of their special properties and testing work put forward. Based on the constitutive relationship between the propagation characteristic of acoustic wave in materials and the surface wave velocity, an acoustic elasticity theoretical model of the surface acoustic waves (SAW) velocities of silicon crystal contacting with its elastic constants is established. The theoretical SAW velocities distribution curves of different crystallographic planes versus azimuthal angles are calculated by using the transformation matrix. Experimental measurements of SAW velocities along different azimuthal angles of three crystallographic planes by using the line focusing acoustic transducer, the high-precision defocusing measurement system and V(f, z) analysis, and the experimental curves of SAW velocities are consistent with the theoretical values. It proves that acoustic microscopy (AM) technology is of highly accuracy and reliability for the SAW velocities measurements of anisotropic materials. Meanwhile, the corresponding consistency between the crystal structure and SAW velocities of silicon crystal is studied further, which establishes the theoretical basis for the property detections and evaluations of anisotropic materials including silicon crystal.

参考文献

[1] 唐见茂. 航空航天材料发展现状及前景[J]. 航天器环境工程, 2013, 30(2):115-121. TANG Jianmao. A review of aerospace materials[J]. Spacecraft Environment Engineering, 2013, 30(2):115-121.
[2] 钱元, 周光明, 蔡登安, 等. 双轴向纤维增强复合材料层合板强度准则[J]. 南京航空航天大学学报, 2013, 45(2):179-185. QIAN Yuan, ZHOU Guangming, CAI Dengan, et al. Investigation of strength criterion for biaxial fiber-reinforced composite laminated plates[J]. Journal of Nanjing University of Aeronautics & Astronautics, 2013, 45(2):179-185.
[3] 王习术, 李春. 材料各向异性力学行为试验研究方法探讨[J]. 试验技术与试验机, 2006, 46(4):1-7. WANG Xishu, LI Chun. An investigation of testing methods on the biaxial mechanical behaviors of anisotropic materials[J]. Test Technology and Testing Machine, 2006, 46(4):1-7.
[4] 王红美, 徐滨士, 马世宁, 等. 纳米压痕法测试电刷镀镍镀层的硬度和弹性模量[J]. 机械工程学报, 2005, 41(4):128-131. WANG Hongmei, XU Binshi, MA Shining, et al. Hardness and modulus of elasticity of brush plated nickle coating by nanoindentation testing[J]. Chinese Journal of Mechanical Engineering, 2005, 41(4):128-131.
[5] 陈樟, 苏伟, 万敏. 单晶硅纳米压痕过程的有限元模拟与试验验证[J]. 微纳电子技术,2009, 46(2):104-107. CHEN Zhang, SU Wei, WAN Min. FEM simulation and experiment verification of the monocrystal silicon nanoindentation process[J]. Micronanoelectronic Technology, 2009, 46(2):104-107.
[6] 李东升, 杨德仁, 阙端麟. 单晶硅材料机械性能研究及进展[J]. 材料科学与工程,2000,18(3):100-104. LI Dongsheng, YANG Deren, QUE Duanlin. Progress in study of crystal silicon mechanical properties[J]. Journal of Materials Science and Engineering, 2000, 18(3):100-104.
[7] 李德刚, 梁迎春, 白清顺. 单晶硅各向异性力学性能纳米压痕试验研究[J]. 航空精密制造技术,2008, 44(2):9-12. LI Degang, LIANG Yingchun, BAI Qingshun. Nano-indentation experiments on anisotropic mechanical properties of single crystal silicon[J]. Aviation Precision Manufacturing Technology, 2008, 44(2):9-12.
[8] 张泰华, 杨业敏, 赵亚溥, 等. MEMS材料力学性能的测试技术[J]. 力学进展, 2002, 32(4):545-562. ZHANG Taihua, YANG Yemin, ZHAO Yapu, et al. Measurement of mechanical properties of MEMS materials[J]. Advances In Mechanics, 2002, 32(4):545-562.
[9] 陈倩栎, HERRMANN K, MENELAO F. 纳米压痕仪和激光超声技术检测薄膜弹性模量[J].中国测试技术,2007, 33(1):77-81. CHEN Qianli, HERRMANN K, MENELAO F. Comparative study about the determination of the Young's modulus of thin layers with the instrumented indentation test and the laser-acoustic measuring method[J]. China Measurement & Test, 2007, 33(1):77-81.
[10] 陆铭慧, 杨奕, 陈以方, 等. 声学法测量复合绝缘子弹性常数[J]. 材料工程, 2005(11):46-49. LU Minghui, YANG Yi, CHEN Yifang, et al. Determination of elastic constants in composite insulator from ultrasonic method[J]. Journal of Materials Engineering, 2005(11):46-49.
[11] WANG S F, HSU Y F, Pu J, et al. Determination of acoustic wave velocities and elastic properties for diamond and other hard materials[J]. Materials Chemistry and Physics, 2004, 85(2-3):432-437.
[12] KUSHIBIKI J I, OHASHI Y, ARAKAWA M, et al. Procedures for determining acoustical physical constants of class 6mm single crystals by ultrasonic microspectroscopy technology[J]. Journal of Applied Physics, 2009, 105(11):114913-1-114913-9.
[13] KIM J O, ACHENBACH J D, MIRKARIMI P B, et al. Elastic constants of single-crystal transition-metal nitride films measured by line-focus acoustic microscopy[J]. Journal of Applied Physics, 1992, 72(5):1805-1811.
[14] 何存富, 刘岳鹏, 刘增华, 等. 空气耦合Lamb波在单晶硅中的传播特性和缺陷检测研究[J]. 机械工程学报, 2015, 51(12):1-7. HE Cunfu, LIU Yuepeng, LIU Zenghua, et al. Air-coupled Lamb waves propagation characteristics and defect detection in monocrystalline silicon[J]. Journal of Mechanical Engineering, 2015, 51(12):1-7.
[15] 宋国荣, 何存富, 黄垚, 等. 小试件材料弹性常数超声测量线聚焦探头的研制[J]. 仪器仪表学报, 2008, 29(11):2298-2303. SONG Guorong, HE Cunfu, HUANG Yao, et al. Design of line-focus PVDF ultrasonic transducer for elastic constant measurement of limited-size samples[J]. Chinese Journal of Scientific Instrument, 2008, 29(11):2298-2303.
[16] 宋国荣,吕炎,谭博涛,等. 薄板涂层结构镀镍层声学特性检测与弹性常数反演表征方法研究[J]. 机械工程学报. 2014, 50(4):11-17 SONG Guorong, LÜ Yan, TAN Botao, et al. Research on measurements of acoustic characteristics of nickel-coating plate and inversion method of elastic constants[J]. Journal of Mechanical Engineering, 2014, 50(4):11-17
[17] LÜ Yan, HE Cunfu, SONG Guorong, et al. Elastic properties inversion of an isotropic plate by hybrid particle swarm-based-simulated annealing optimization technique from leaky Lamb wave measurements using acoustic microscopy[J]. Journal of Nondestructive Evaluation, 2014, 33:651-662.
[18] NAYFEH A H, ANDERSON M J. Wave propagation in layered anisotropic media with applications to composites[J]. Journal of the Acoustical Society of America, 2000, 108:471-472.
文章导航

/