Xiang Hongliang, Shen Lixiang, Deng Liping
The effects of different annealing temperature and time on the microstructural evolution and mechanical properties of the oxygen free copper tube were investigated by OM, TEM, SEM and universal tensile tester.The results reveal that:the high energy and high density dislocation of the as-deformed sample are evolved into thin dislocation walls, subgrain boundaries and then high angle grain boundaries with annealing at 260℃ or 300℃ for 60min, resulting in low density dislocation structure. After annealing at 300℃, recovery and recrystallization are fully completed.The tensile strength, yield strength and hardness are decreased with temperature increase, while the elongation is increased.Within the annealing temperature range of 300℃ to 460℃, the change of mechanical properties of the copper tube can be ignored.Increasing the annealing time at 300℃ from 10min to 60min, recrystallization is induced gradually, and the tensile strength, yield strength and hardness are decreased, while elongation is increased.With annealing for 60min, recrystallization is finished, and the tensile fracture morphology is changed from quasi-cleavage surface, tearing edge and dimple characteristics to equiaxial dimples. Compared with those of as-deformed sample, the tensile strength, yield strength and hardness of the copper tube are decreased by 39%, 68.5% and 53.1%, respectively, and the elongation is increased from 1.2% to 50%.With annealing time more than 60min, the grain size is increased slightly before reached a stable value, showing an insignificant effect on the mechanical properties.