交叉与前沿

微细多孔结构内两相驱替试验研究

  • 孙川翔 ,
  • 高诚 ,
  • 黄峰
展开
  • 1. 中国石化石油勘探开发研究院 北京 100083;
    2. 清华大学能源与动力工程系 北京 100084
孙川翔,女,1990年出生,工程师。主要研究方向为页岩气勘探开发相关的试验和数值模拟。E-mail:suncx.syky@sinopec.com;黄峰,男,1993年出生,博士研究生。主要研究方向为微尺度多孔介质内的两相流动。E-mail:thuhuangfeng@163.com

收稿日期: 2017-09-06

  修回日期: 2018-01-30

  网络出版日期: 2018-08-20

Experimental Study on Two Phase Flow in Micro Scale Porous Structure

  • SUN Chuanxiang ,
  • GAO Cheng ,
  • HUANG Feng
Expand
  • 1. Petroleum Exploration and Production Research Institute, SINOPEC, Beijing 100083;
    2. Department of Energy and Power Engineering, Tsinghua University, Beijing, 10084

Received date: 2017-09-06

  Revised date: 2018-01-30

  Online published: 2018-08-20

摘要

利用等离子体干法刻蚀硅片制作微细尺度多孔结构模型,采用倒置荧光共聚焦显微镜作为跟踪观测手段,去离子水为润湿相,十二烷为非润湿相构成多组分两相流体。试验研究微细多孔结构内两相驱替规律,发现液桥、锥状液滴、液膜等存在于多孔介质表面的多种形式。试验结果表明:十二烷驱替去离子水的排驱过程中,随着毛细数的增大,十二烷的饱和度逐渐增大。去离子水倾向于以液桥的形式稳定地占据尺寸较小的孔喉部位,十二烷倾向于占据尺寸较大的孔身部位。去离子水驱替十二烷的吸吮过程中,优势通道多集中在微观模型的边壁区域,更容易形成优势通道达到突破状态,从而很快地达到稳定的两相相态分布,十二烷以圆锥状的形式附着在多孔结构圆柱表面,说明圆锥状液滴的存在与初始的饱和相态有关。

本文引用格式

孙川翔 , 高诚 , 黄峰 . 微细多孔结构内两相驱替试验研究[J]. 机械工程学报, 2018 , 54(16) : 227 -232 . DOI: 10.3901/JME.2018.16.227

Abstract

Micro scale porous structure is manufactured through plasma reaction method. The inversed fluorescence microscope is utilized to track and analysis two-phase interface, with deionized water and dodecane designed as wetting phase and non-wetting phase fluid respectively. The reliability of the experimental system is verified and various profiles such as fluid bridge, cone-shaped droplet and fluid film are observed lying on the surface of porous media during the two-phase displacement process. The results showthat:during the drainage process, the saturation of dodecane will increase when the value of Capillary number climbs up. Deionized water tended to occupy the pore throats with smaller size while dodecane is more inclined to take up larger pores. In contrast, during the imbibition progress, the dominant migration pathways are usually distributed at the side wall areas of the micro scale porous structure, which are conducive for the fluid to break though and reach a stable distribution of the two phases. Dodecane stuck to the surface of the porous structure shaped like a cone. Thus, the presence of the cone-shaped droplets are related to the initial saturation phase.

参考文献

[1] 高诚, 胥蕊娜, 姜培学. 超临界CO2 在地下盐水层内弥散现象的数值模拟[J]. 清华大学学报, 2015, 55(10):1105-1116. GAO Cheng, XU Ruina, JIANG Peixue. Numerical simulation of the dispersion of supercritical CO2 storage in saline aquifers[J]. Journal of Tsinghua University, 2015, 55(10):1105-1116.
[2] BACHU S. CO2 storage in geological media:role, means, status and barriers to deployment[J]. Progress in Energy and Combustion Science, 2008, 34:254-273.
[3] 周军平, 鲜学福, 姜永东, 等. 不可采煤层CO2 封存的数值模拟[J]. 重庆大学学报, 2011, 34(7):83-90. ZHOU Junping, XIAN Xuefu, JIANG Yongdong, et al. Numerical simulation of carbon dioxide storage in unmineable coalbed[J]. Journal of Chongqing University, 2011, 34(7):83-90.
[4] 董华松, 黄文辉. CO2 捕捉与地质封存及泄漏监测技术现状与进展. 资源与产业, 2010, 12(2):123-128. DONG Huasong, HUANG Wenhui. Research of CO2 capture, geological, storage and leakage technologies. Resources & Industries, 2010, 12(2):123-128.
[5] XU R N, JIANG P X. Numerical simulation of fluid flow in microporous media. International Journal of Heat and Fluid Flow, 2008, 29(5):4418-4424.
[6] 高诚, KANG Qinjun, 胥蕊娜, 等. 基于二氧化碳封存的超临界两相流动的数值研究[J]. 工程热物理学报, 2015, 55(10):1105-1116. GAO Cheng, KANG Qinjun, XU Ruina, et al. The numerical investigation of supercritical two phase fluid flow in support of carbon dioxide storage[J]. Journal of Engineering Thermophysics, 2014, 35(5):944-947.
[7] GAO Cheng, XU Ruina, JIANG Peixue. Pore-scale numerical investigation of fluid flow in porous media using lattice Boltzmann method[J]. International Journal of Numerical Methods for Heat & Fluid Flow, 2015, 25(8):1957-1977.
[8] 姚军, 孙海, 黄朝琴, 等. 页岩气藏开发中的关键力学问题. 中国科学:物理学力学天文学, 2013, 43(12):1527-1547. YAO Jun, SUN Hai, HUANG Zhaoqin, et al. Key mechanical problems in the development of shale gas reservoirs[J]. Science China Physics:Mechanica & Astronomica, 2013, 43(12):1527-1547.
[9] BOEK E S, VENTUROLI M. Lattice-Boltzmann studies of fluid flow in porous media with realistic rock geometries[J]. Computers & Mathematics with Applications, 2010, 59:2305-2314.
[10] 贾承造, 郑民, 张永峰. 中国非常规油气资源与勘探开发前景[J]. 石油勘探与开发, 2012, 39(2):129-136. JIA Chengzao, ZHENG Min, ZHANG Yongfeng. Unconventional hydrocarbon resources in China and the prospect of exploration and development[J]. Petroleum Exploration and Development, 2012, 39(2):129-136.
[11] CHEN Li, CAO Taofeng, LI Zhaohui, et al. Numerical investigation of liquid water distribution in the cathode side of proton exchange membrane fuel cell and its effects on cell performance[J]. International Journal of Hydrogen Energy, 2012, 37(11):9155-9170.
[12] LENORMAND R; TOUBOUL E, ZARCONE C. Numerical models and experiments on immiscible displacements in porous media[J]. Fluid Mech., 1988, 189:165-187.
[13] PILLER M, SCHENA G, NOLICH M, et al. Analysis of hydraulic permeability in porous media:from high resolution X-ray tomography to direct numerical simulation[J]. Transp. Porous Med., 2009, 80:57-78.
[14] 马瑾, 胥蕊娜, 罗庶, 等. 超临界压力CO2 在深部咸水层中运移规律研究[J]. 工程热物理学报, 2012, 33(11):1971-1975. MA Jin, XU Ruina, LUO Shu, et al. Core-scale experimental study on supercritical-pressure CO2 migration mechanism during CO2 geological storage in deep saline aquifers[J]. Journal of Mechanical Engineering, 2012, 33(11):1971-1975.
[15] XU Shaolin, SHIMADA K, MIZUTANI M, et al. Analysis of machinable structures and their wettability of rotary ultrasonic texturing method[J]. Chinese Journal of Mechanical Engineering, 2016, 29(6):1187-1192.
[16] LUO S, XU Ruina, JIANG Peixue, et al. Visualization experimental investigations of supercritical CO2 inject into porous media with the fissure defect[J]. Energy Procedia, 2011, 4:4411-4417.
[17] 吴楠, 张显程, 涂善东, 等. 室温和650℃下晶粒尺寸对GH4169合金疲劳小裂纹萌生和扩展行为的影响[J]. 机械工程学报, 2016, 52(20):66-75. WU Nan, ZHANG Xiancheng, TU Shandong, et al. Grian size effect on the initiation and propagation of small fatigue crack of GH4169 alloy at room temperature and 650℃[J]. Journal of Mechanical Engineering, 2016, 52(20):70-76.
[18] 赵爽, 赵子华, 雷鸣, 等. 微米尺度铜键合丝疲劳性能研究[J]. 机械工程学报, 2016, 52(18):71-76. ZHAO Shuang, ZHANG Zihua, LEI Ming, et al. Research on fatigue properties of micron scale copper bonding wires[J]. Journal of Mechanical Engineering, 2016, 52(18):71-76.
[19] KARADIMITRIOU N K, HASSANIZADEH S M. A review of micromodels and their use in two-phase flow studies[J]. Vadose Zone Journal, 2011, 11(3):vzj20110072.
文章导航

/