20 July 2017, Volume 41 Issue 7
    

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  • CHEN Tao, ZHAO Luyuan, LI Hui, HUANG Jun, WU Yucheng
    Materials For Mechanical Engineering. 2017, 41(7): 1-5,12. https://doi.org/10.11973/jxgccl201707001
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    Stress controlled fatigue tests at different stress amplitudes, 60%, 70%, 80% and 90% of yield strength (σs) of the tested alloy, respectively, were conducted on 7075-T651 aluminum alloy. The cyclic strain response of the alloy was studied, the fatigue fracture morphology, surface damage morphology and microstructure were observed and the initiation and propagation mechanisms of fatigue crack were analyzed. The results show that micro-scale Al7Cu2Fe particles, nano-scale η' (MgZn2) phase and relatively large sized η (MgZn2) phase were precipitated in the tested alloy. Moreover, fine and sphere-like GP zones with size of 3-10 nm were observed. Under the control of relatively high stress amplitude (80%σs,90%σs), the tested alloy showed a fatigue behavior of first softening then hardening until fracture, while first softening then hardening until becoming stable relatively at low stress amplitudes (60%σs, 70%σs). The tested alloy mainly fractured in a micropore gathered dimple manner. At high stress amplitude, fatigue cracks initiated at the coarse inclusion of Al7Cu2Fe and second phase of MgZn2, with dislocation tangling a lot. Whereas at low stress amplitude, the crack source was at the slightly torn position of the substrate, and the produced dislocation showed shapes of dispersed short or long straight dislocation lines.
  • LU Jintao, ZHANG Bo, HUANG Jinyang, YANG Zhen, XU Hongjie
    Materials For Mechanical Engineering. 2017, 41(7): 6-12. https://doi.org/10.11973/jxgccl201707002
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    Corrosion behavior of candidate alloys such as 316L stainless steel, 316Lmod stainless steel, HR3C stainless steel, Inconel718 alloy and TC4 alloy used for critical parts of urea hydrolysis equipment in gas denitrification was studied in simulated urea hydrolysis environment. The results show that different degree of dissolve corrosion was happened for 316L and 316Lmod stainless steel at the initial stage. In the following corrosion stage, corrosion product deposition increased and a large surface of corrosion products exfoliation were observed on 316L stainless steel which was mainly pitting corrosion, while uniform corrosion and deposition of corrosion products dominated the corrosion process for 316Lmod stainless steel. TC4 alloy, Inconel718 alloy and HR3C stainless steel showed a better corrosion resistance compared with 316L and 316Lmod stainless steel. There was a dense titanium oxide layer with 3 μm in thickness formed on surface of TC4 alloy and mixed oxides consisting of Cr2O3 and Fe2O3 formed by hydrothermal synthesis reaction were the main corrosion products. A small amount of dissolve corrosion was observed on Inconel718 alloy at the initial stage and in later stage deposition of corrosion products dominated the corrosion process. Intergranular corrosion was clearly observed in HR3C stainless steel at the initial stage and deposition of corrosion products dominated the following corrosion process of HR3C stainless steel.
  • WANG Lei, LIU Xin, XIE Huanwen, ZOU Liming, CAI Yixiang
    Materials For Mechanical Engineering. 2017, 41(7): 13-17,23. https://doi.org/10.11973/jxgccl201707003
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    The spherical cast tungsten carbide particles with different contents and particle sizes was mixed with atomized Fe powder to prepare surfacing electrodes. The surfacing layer on Q235 steel substrate was obtained using oxygen-acetylene flame surfacing. The effect of content and particle size of spherical cast tungsten carbide on the microstructure, hardness and wear resistance of surfacing layer was investigated. The results show that there was an obvious melting phenomenon at the edges of spherical cast tungsten carbide in surfacing layer. The smaller the particle size of spherical cast tungsten carbide was, the more obvious the melting phenomenon was. The fish-bone ledeburite decreased with decrease of spherical cast tungsten carbide particles content, and the ledeburite became coarser with reduction of particle size of spherical cast tungsten carbide. The more spherical cast tungsten carbide particles content was, and the smaller particle size was, the higher the hardness was and the better the wear resistance of surfacing layer was.
  • RAN Min, YAN Hongge, CHENG Xiangfei, CHEN Jihua, SU Bin, XIA Weijun, ZHANG Ming
    Materials For Mechanical Engineering. 2017, 41(7): 18-23. https://doi.org/10.11973/jxgccl201707004
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    The changes of microstructure, mechanical and damping properties of Fe-17Mn-8Cr alloy during multi-directional forging process were investigated by tensile testing and dynamic thermal mechanical analyzer. The results show that during multi-directional forging process the ε-martensite and γ-austenite plates were greatly refined and more uniformly distributed. Meanwhile, a high density of dislocations was introduced and yield strength was improved obviously. The logarithmic decrement of Fe-17Mn-8Cr alloy after multi-directional forging declined but the alloy still had a high damping capacity. The damping mechanism of this alloy was interaction between the effect of variant crossing degree of ε-martensite on γ/ε interface movement and the effect of high density of dislocations on stacking fault movement.
  • WU Yuemei, ZHOU Liming, XIONG Ji, YE Junliu, WEN Bin
    Materials For Mechanical Engineering. 2017, 41(7): 24-28,33. https://doi.org/10.11973/jxgccl201707005
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    Based on the similar effect of WC and Mo2C addition on microstructure optimizing and wettability improvement of Ti(C,N)-based cermets, the microhardness of Ti(C,N)-based cermets with WC or Mo2C addition was investigated at high temperature. The results show that the high-temperature microhardness of Ti(C,N)-based cermets with WC and Mo2C addition both decreased with the increase of temperature. At 600-800℃, the high-temperature microhardness of cermets containing WC was slightly higher than that of cermets with Mo2C and microhardness was almost the same at 900℃. The indentation area and average indentation depth of two cermets both increased with increase of temperature. The true strain of cermets with WC was significantly less than that of cermets with Mo2C addition, but high-temperature deformations of two cermets were nearly close at 900℃.
  • LIU Huihui, WANG Xin, OUYANG Jindong, YI Long, HAO Chuanhai, ZHANG Bo
    Materials For Mechanical Engineering. 2017, 41(7): 29-33. https://doi.org/10.11973/jxgccl201707006
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    Micro-bending tests were conducted by RG-2000 micro-computer control electronic universal testing machine. The influence of thickness, grain size, bending radius of C5210 phosphor bronze sheet on micro-bending spring-back was researched. Results show that the thickness, grain size, bending radius of C5210 phosphor bronze sheet had a significant effect on the spring-back and that showed an obvious size effect. The spring-back amount decreased as sheet thickness increased, and thickness affected the spring-back amount obviously. The spring-back amount decreased with increasing of grain size, when the grain size was larger than 40 μm, the amount of spring-back decreased slowly. The spring-back amount increased as the bending radius increased, and the trend of increase was more obvious when the thickness of sheet was smaller.
  • WANG Guojian, SUN Yaoning, WANG Xiaoning, JIANG Wanle
    Materials For Mechanical Engineering. 2017, 41(7): 34-38,42. https://doi.org/10.11973/jxgccl201707007
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    Artificial UV irradiation aging test under warm-wet environment was conducted for glass fiber reinforced unsaturated polyester resin composite. The effect of UV aging on mass loss rate, barcol hardness, tensile and bending mechanical properties and their failure patterns of composite was studied. The structure and micro morphology were analyzed. Results show that the mass loss rate of composite increased continuely with the increase of UV aging time.The barcol hardness of the irradiated surface was lower than that of non-irradiation surface, and the retained rate of barcol hardness increased first and then dedecreased with the increase of UV aging time. The tensile and bending strength of composite were improved first and then decreased slowly. Cavity density and tenacity white stripe in composite after aging increased, and it presented obvious lamellar wave pattern. Repture of chemical bonds took place in composite and UV irradiation made the structure changed.
  • LI Tuo, BAI Hongbai, LU Chunhong
    Materials For Mechanical Engineering. 2017, 41(7): 39-42. https://doi.org/10.11973/jxgccl201707008
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    Based on the theory of locally resonance, a kind of composite which contained metal rubber as basic framework, acid sillcone as matrix and plumbum balls as scatterer was designed. The influences of composite parameters (filling rate of metal wires, diameter of small plumbum balls, filling rate of small plumbum balls) and thickness of air layer behind composite on low-frequency sound absorption property of metal rubber composite was studied by sound absorption tests. The results show that metal rubber composite had the excellent low-frequency sound absorption property. The reduction of filling rate of metal wires, increase of diameter and filling rate of plumbum balls all could improve the low-frequency absorption property of composite. With increase of air layer thickness, the frequency of the resonant sound absorption moved towards the direction of low-frequency.
  • CAI Xiang, ZHANG Hui, CHEN Shuang
    Materials For Mechanical Engineering. 2017, 41(7): 43-48,53. https://doi.org/10.11973/jxgccl201707009
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    The SiCp/Al composites with SiC volume fraction of 30%, 40% and 50% were prepared by powder extrusion forming. The microstructure, mechanical properties and physical properties of different SiCp/Al composites were analyzed by optical microscopy, scanning electron microscopy, tensile tester, brinell hardness tester, thermodilatometer and thermal conductivity detector. The results showed that 30% and 40% SiCp/Al composites could be extruded in 450℃, but 50% SiCp/Al composite failed. On longitudinal section of composite, the aluminum matrix was distributed along the extrusion direction and presented the white strip streamline structure. The tensile fracture surface of two composites was made up of a large number of smaller dimples, both of which presented mixed fracture characteristics. With increase of SiCp volume fraction, the brinell hardness increased from 81.9 HB to 98 HB while tensile strength decreased slightly and the elongation reduced obviously. The relative density and coefficient of linear expansion of the composite reduced while thermal conductivity improved.
  • JI Shuai
    Materials For Mechanical Engineering. 2017, 41(7): 49-53. https://doi.org/10.11973/jxgccl201707010
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    High silicon electrical steel ingot with three-layer structure was prepared by clad casting using common silicon steel and silicon ferrosilicon alloy, then 6.5%Si electrical steel composite plate was obtained by traditional rolling process and diffusion annealing process. Microstructure and Si element distribution were studied by optical microscope and scanning electrical microscope. Magnetic properties were also tested. The results show that electrical steel composite plate with 0.5 mm thickness could be prepared by this method successfully. After 1 200℃×75 min diffusion annealing treatment, Si element diffused completely and three layers of composite plate was changed into single layer gradually, while the content of Si element was about 6.5wt.%. The value of iron loss P1.5/50 was 2.68-2.72 W·kg-1 and the values of magnetic induction B8 was 1.370-1.378 T, B50 was 1.610-1.625 T for 6.5%Si electrical steel composite plate. Compared with Fe-6.5%Si alloy whose thickness was 0.34 mm, 6.5%Si electrical steel composite plate prepared by this method had a higher magnetic induction but greater iron loss.
  • QUE Wumei, HUANG Youting, CHEN Wenzhe
    Materials For Mechanical Engineering. 2017, 41(7): 54-59,65. https://doi.org/10.11973/jxgccl201707011
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    CuW80 alloy was prepared by infiltration sintering method, then the gradient structure copper-tungsten based carbide composite was obtained by carburizing process for 4 h at 1 250℃. The compression tests for alloys before and after carburizing were carried out on universal testing machine at different temperatures, and microstructure and compression fracture were observed by scanning electron microscope. Effect of temperature on compression performance for composite was researched, and the failure mechanism was analyzed. The results show that a carburization layer with 70 μm thickness was formed on the surface of composite and surface hardness was improved by 95.1% compared with that of CuW80 alloy. There was a significant work hardening process for composite during room temperature compression process, but the hardening effect gradually weakened as temperature increased. The compressive strength and compression ratio declined as temperature increased. The compression property of composite was better than that of CuW80 alloy. Fracture morphology of composite mainly included dimples and then mostly plastic holes as temperature increased, and compression fracture failure mode was brittle fracture mixed with ductile fracture.
  • ZENG Bin, LIU Wanfeng, ZENG Wujun, CHEN Dan, XIA Qiuying
    Materials For Mechanical Engineering. 2017, 41(7): 60-65. https://doi.org/10.11973/jxgccl201707012
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    Carbon nanotubes and reduced graphene oxides with CuO (CNTs/rGO-CuO) composite powder was synthesized by spray drying and post-calcinating method, and the phase and morphology were analyzed. The synthesis conditions that had a significant effect on the morphology and photocatalytic performance of composite powder such as decomposed temperature, carbon nanotubes (CNTs) to graphene oxides (GO) mass ratio, CNTs and GO mass fraction were discussed. The preparation process was optimized. The results show that when the decomposed temperature was 210℃, CNTs to GO mass ratio was 1:1, CNTs and GO mass fraction was 10%, the composite powder had the best property. CNTs and rGO formed a spherical structure and CuO particles were uniformly distributed on the surface of the spherical structure. 98.3% degradation of methyl orange (MO) could be obtained after 20 min under visible light.
  • SHI Bowen, JIANG Yingjie, SUN Qingchao
    Materials For Mechanical Engineering. 2017, 41(7): 66-69,75. https://doi.org/10.11973/jxgccl201707013
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    The super high cycle fatigue property of FV520B-I steel was studied by ultrasonic and conventional fatigue test method with frequency of 20 kHz and 140 Hz, respectively. The influence of loading frequency on super high cycle fatigue property of FV520B-I steel was investigated, and the ultrasonic fatigue testing data was corrected based on Basquin formula. The results show that the fatigue life of FV520B-I steel increased with increase of loading frequency when stress amplitude was the same, while fatigue strength was decreased. The fatigue fracture mechanism and fracture morphology of FV520B-I steel in ultrasonic fatigue test were almost the same with that in conventional fatigue test. The corrected ultrasonic fatigue test data had a good compatibility with conventional fatigue test data.
  • LIU Jihua, CHEN Shuiyou, LIU Qiyue
    Materials For Mechanical Engineering. 2017, 41(7): 70-75. https://doi.org/10.11973/jxgccl201707014
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    The friction and wear behavior between the wheel steels with four chemical composition and hot-rolled U71Mn rail steel was studied using a wheel/rail wear tester, and the effects of wheel steel composition and hardness on the wear behavior and wear mechanism were analyzed. The results show that with the increase of carbon content, the proeutectoid ferrite content reduced obviously, the pearlitic grain size increased, and the thickness of cementite lamella also increased in the microstructure of the wheel steel, resulting in the increase of wheel steel hardness. With the increase of wheel steel hardness, the wear loss of the wheel steel decreased and the main wear mechanism changed from abrasive wear and shallow delamination wear into deep delamination wear, while the wear loss of the rail steel increased and the main wear mechanism was shallow delamination wear.
  • ZHAO Xin, SHAN Aidang
    Materials For Mechanical Engineering. 2017, 41(7): 76-79,84. https://doi.org/10.11973/jxgccl201707015
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    Ultrafine-grained Ni-based alloy was prepared by 98% severe deformation with combination of asymmetric-rolling and symmetric-rolling. The microstructure and tensile properties of the alloy after annealing were studied. The results show that the structure of Ni-based alloy was significantly refined after rolling and the grain size was less than 200 nm and 300 nm after annealing at 700℃ and 800℃, respectively. It was found that the ultrafine-grained Ni-based alloy had a good structure stability. The strength of Ni-based alloy was significantly improved after rolling and remained very high after annealing at 700℃ and 800℃. Especially after annealing at 700℃, the yield strength and tensile strength were increased from 243 MPa and 679 MPa to 1 907 MPa and 1 949 MPa, respectively. The strength improvement and good structure stability of ultrafine grain Ni-based alloy were mainly attributed to a large amount of uniformly dispersed nano-sized γ' phase that precipitated during annealing process.
  • BI Zongyue, YAN Peilin, WANG Haitao, YU Han
    Materials For Mechanical Engineering. 2017, 41(7): 80-84. https://doi.org/10.11973/jxgccl201707016
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    The microstructure and formability of weld for 16Cr stainless steel plate with 3.4 mm thickness by high frequency welding method in different welding parameters were studied, and the welding process was optimized. Then the properties of 16Cr stainless steel welded pipe joint under optimized process were studied by tensile test, flattening test and flaring test. The results show that welded joint with excellent formability was obtained when welding speed was 10 m·min-1 and welding heat input was 3.0 kJ·cm-1. The microstructure of weld was composed of austenite and δ-ferrite. Although the welded pipe had high strength, the toughness got worse due to the presence of oxide inclusions in the weld. The oxide inclusion in the weld could be effectively reduced by application of appropriate gas protection and avoiding high temperature weld contacted with water.
  • FENG Qingfeng, YAO Zaiqi, YE Tuo, ZHU Ling, WANG Zhenhu, GUO Pengcheng, LI Luoxing
    Materials For Mechanical Engineering. 2017, 41(7): 85-90,97. https://doi.org/10.11973/jxgccl201707017
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    Dynamic compression test of 6013-T4 aluminum alloy was conducted by split Hopkinson pressure bar apparatus at different temperatures (25, 200, 300℃) and strain rates (1 000, 2 000, 3 000, 4 000, 5 000 s-1), and dynamic mechanical behavior under impact load was investigated. Numerical simulation of dynamic impact experiment was carried out by the fitted Johnson-Cook constitutive equation. The results show that 6013-T4 aluminum alloy had significant strain rate and strain hardening effect, and the dynamic flow stress decreased with increase of deformation temperature. The yield strength at room temperature was insensitivity to strain rate. As deformation temperature increased, the strain rate sensitivity of yield strength gradually increased. Based on the quasi-static at room temperature and dynamic true stress-true strain curves at different temperatures and strain rates, Johnson-Cook constitutive equation of the alloy was determined. The simulated results of true stress-true strain curves at different temperatures and strain rates were consistence with the experimental and constitutive results.
  • DING Zhiping, FAN Kai, ZHANG Yaxin, LI Zaike, WANG Jiashi, ZENG Jiaxing
    Materials For Mechanical Engineering. 2017, 41(7): 91-97. https://doi.org/10.11973/jxgccl201707018
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    Based on micro-mechanics Mori-Tanaka method of composite, macroscopic elastic constants of composite predicted by Digimat software and the response coupling relationship between micro-and macro-mechanics for composite was established. Considering manufacturing defects of composite, the method of reverse regression iteration was employed to modify elastic constants of matrix material. Based on the computing platform coupled ABAQUS software with Digimat software, Mori-Tanaka micro-mechanics constitutive model was called in the finite element model of composite leaf spring and micro-mechanics damage of composite was considered, then the numerical simulation of macro-micro multiscale coupling progressive failure was implemented by introducing the fiber and matrix failure criteria which realized ultimate load prediction of composite leaf spring and was validated by ultimate load test of composite leaf spring. The results show that the test fracture location of composite leaf spring consistent with that of simulated prediction, and deviation between test and prediction values of ultimate load was only 5.1%.
  • LI Shikang, LI Luoxing, XU Rong
    Materials For Mechanical Engineering. 2017, 41(7): 98-104,110. https://doi.org/10.11973/jxgccl201707019
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    The temperature rise of 6063 aluminum alloy during hot compression was studied by hot compression test conducted on Gleeble-1500 thermal simulator with strain rates of 0.01-10 s-1 at 400-520℃. Considering the effect of heat conduction and heat radiation, the influence of deformation temperature, strain rate and strain on the adiabatic correction factor were investigated and the equation of material deformation temperature rise was optimized. The temperature rise during hot compression at medium strain rates was corrected. The results show that adiabatic correction factor decreased with the increase of strain. The higher deformation temperature and strain rate were, the greater adiabatic correction factor was. Heat conduction and heat radiation had a significant influence on temperature rise during alloy deformation. The deformation temperature rise after correction had a nonlinear relationship with strain. Temperature changing curve calculated was almost the same with that measured and the average error was less than 3%.
  • TIAN Xiao, XU Hui, QIN Chengpeng, WANG Libo, CAO Jianfeng, LI Yimin
    Materials For Mechanical Engineering. 2017, 41(7): 105-110. https://doi.org/10.11973/jxgccl201707020
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    The circumferential cracking reason of 15CrMoG steel connecting tube of transition-section water wall during installation stage had been analyzed by macroscopic examination, chemical composition analysis, mechanical property testing, microstructure observation and fracture appearance analysis. The results show that the great stress concentration occurred in incomplete penetration of fillet weld at tail of fin after butt-weld, microstructure contained martensite+bainite hardening structure and hardness was extremely high. The pipeline restraint stress and welding residual stress caused the crack initiation from this location. Base metal of the area had high hardness and low plasticity and the crack expanded along the tube circumference under the transverse tension stress, which resulted in the brittle cracking of tube at the circumferential direction.