20 June 2017, Volume 41 Issue 6
    

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  • YE Tuo, LI Luoxing, TANG Xu, HAO Wenjing, TANG Ming, LI Rongqi
    Materials For Mechanical Engineering. 2017, 41(6): 1-4. https://doi.org/10.11973/jxgccl201706001
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    The effects of solid solution at different temperatures (505-555℃) for 1 h and aging at 180℃ for different times (2-20 h) on the microstructure and dynamic mechanical behavior of the extruded 6013 Al alloy were investigated by Vickers hardness tester, transmission electron microscope and split Hopkinson pressure bar. The results show that with the solid solution temperature increasing, the hardness and true stress of the alloy during dynamic deformation first increased then decreased. After solid solution at 545℃, both the hardness and the true stress were the largest. With the aging time increasing, the hardness and true stress of the alloy also first increased then decreased. After aging for 8 h, the number of needle-like precipitates in the tested alloy was the largest and the precipitates distributed evenly; the hardness and the true stress also reached the largest values; the difference value between true stresses at the true strain of 0.2 under relatively high (5 000 s-1) and relatively low (2 000 s-1) strain rates was the largest, showing an obvious strain rate sensitivity.
  • ZHANG Min, ZHANG Ming, LU Xiaokang, SHU Shaoyan, LI Jihong
    Materials For Mechanical Engineering. 2017, 41(6): 5-9. https://doi.org/10.11973/jxgccl201706002
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    The Ni and Cr elements were added in CaF2-SiO2-TiO2-CaO base powder with Ni to Cr mass ratio of 1:1, 2:1, 3:1, respectively, then the self-shield flux cored wires were prepared with 2205 stainless steel strip as wrapping material. Using the prepared welding wires, 2205 duplex stainless steel was arc welded, and the effects of Ni to Cr mass ratio on the microstructure and mechanical properties of the weld seam were studied. The results show that with the increase of Ni to Cr ratio, the austenite phase content in the weld seam increases, the ferrite phase content decreases and the size of austenite phase increases. Without the addition of Ni and Cr elements, the strength of the weld seam was the largest while the plasticity was the lowest, and the impact energy was the smallest, which was 72 J. With the increase of Ni to Cr ratio, the strength of the weld seam decreases while the plasticity and impact energy increase. When the mass ratio of Ni to Cr was 3:1, the impact energy of the weld seam had the highest value of 150 J.
  • YANG Yang, YU Chun
    Materials For Mechanical Engineering. 2017, 41(6): 10-13. https://doi.org/10.11973/jxgccl201706003
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    Two electroplated Cu substrates were prepared at current densities of 1.7 mA ·cm-2 and 50 mA ·cm-2. Then by reflow soldering the electroplated Cu substrates and Sn granular, the Sn/Cu joints were obtained and aged at 150℃ for different times (10, 20 d). The surface morphology of the electroplated Cu substrates and interface morphology of the Sn/Cu joints were observed and the evolution mechanism of Kirkendall voids during aging was also analyzed. The results show that after the aging treatment, the voids were formed at Cu3Sn/Cu interface of the two Sn/Cu joints and the density of voids increased gradually with the expansion of aging time and was relatively high at a relatively high current density. Before aging treatment, the voids appeared at the interface of the joint with the electroplated Cu substrate prepared at a relatively high current density; after aging treatment, the voids aggregated gradually and then changed into cavities. The inner surface of cavities became the channels for the rapid diffusion of Cu. The microstructure of the surface electroplate layer was influenced by the current density, which in turn influenced the interfacial microstructure in the following aging process.
  • JIANG Zhihong, WANG Baoyu, GONG Yaoteng, HUANG Xinjian
    Materials For Mechanical Engineering. 2017, 41(6): 14-16. https://doi.org/10.11973/jxgccl201706004
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    Using a vibration tensile tester, the vibration tensile tests under different frequency and excitation force were conducted on Q235A steel. The effects of frequency and excitation force on the average load and yield strength of the steel were studied. The results show that comparing to those in regular tensile, both the average load and yield strength of the tested steel decrease in the vibration tensile, indicating an obvious volume effect. With the increase of excitation force, the yield strength and average load in different deformation stages of the tested steel decrease linearly. With the frequency decreasing, the yield strength and average load in different deformation stages first increases then decreases and reaches the largest value at 90 Hz.
  • SHENG Wei, LIU Tianqi, MA Shaojun, CHEN Tianyun
    Materials For Mechanical Engineering. 2017, 41(6): 17-19. https://doi.org/10.11973/jxgccl201706005
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    The fatigue crack growth rate test was conducted on 300M steel in air atmosphere and 3.5wt% NaCl-water solution, and the fatigue crack growth rate-stress intensity factor range curves were obtained and fitted using Paris and Walker formulas, respectively. The effects of stress ratio, corrosion environment and frequency on the fatigue crack growth rate were analyzed. The results show that the fatigue crack growth rate of 300M steel increased with the increasing stress ratio; at the same stress ratio, the crack growth rate of 300M steel in NaCl-water solution was higher than that in air atmosphere during the early stage of crack growth, and tended to be the same in the later propagation stage; in the early stage of crack growth, the crack growth rate of 300M steel under relatively low frequency was higher than that under relatively high frequency.
  • ZHANG Sa
    Materials For Mechanical Engineering. 2017, 41(6): 20-24. https://doi.org/10.11973/jxgccl201706006
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    Lanthanum-doped lead zirconate titanate (PLZT) ferroelectric ceramics with average grain size of 5 mm and a tetragonal structure were prepared by the conventional solid state reaction method, and then were surface coated with silver and pre-polarized in tangential direction. Then a groove was etched in the silvered surface of the ceramics, sbsequently Vickers indentation was introduced on the groove surface and external electric field was applied along the pre-polarization direction. The domain switching at different positions near the indentation crack tips were in-situ observed by Raman spectroscopy. The variation of the peak intensity of Raman soft modes of E(2TO) and E(3TO+2LO)+B1 versus the observation point was analyzed. The results show that the electric induced strain and 90° domain switching occurred at crack tips under the external electric field. The peak intensity of Raman spectrum and soft modes of E(2TO) and E(3TO+2LO)+B1 decreased with the distance between observation point and crack tip increasing.
  • MA Yonglin, ZHAO Nana, LIU Baozhi, ZHANG Hao, ZHAO Jian, ZHANG Lei, XING Shuqing
    Materials For Mechanical Engineering. 2017, 41(6): 25-29. https://doi.org/10.11973/jxgccl201706007
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    The evolution of microstructure and texture of common grain-oriented silicon steel, which was captured from different processes during cold rolling and annealing, was analyzed by the optical microscope, scanning electron microscope, X-ray diffractometer, etc. The results show that after first cold rolling and decarburizing annealing at 850℃ for 6 min, in the grain-oriented silicon steel the primary recrystallization occurred and the grains transformed from fibrous structure into equiaxed structure with the average grain size of 25 μm. The textures mainly consisted of {001}<010>, {111} <112>, Goss texture, and so on. After the second cold rolling, the grains became smaller in size and transformed into fibrous structure once again. The textures mainly consisted of α texture and γ texture. After annealing at 1 170℃, the second recrystallization occurs in the grain-oriented silicon and the first recrystallization grains grew abnormally, reaching the centimeter level in size. After drawing planishing annealing, the grains became smoother and more homogeneous with the average grain size of 2.28 cm. The orientation density of Goss texture reached the maximum degree of 24.
  • CHEN Guoliang, CHEN Minghe, WANG Ning, SUN Jiawei, WANG Chunyan
    Materials For Mechanical Engineering. 2017, 41(6): 30-33. https://doi.org/10.11973/jxgccl201706008
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    A hot forming process with synchronous cooling followed by aging treatment was conducted on 7075 aluminum alloy in H18 temper, and then the macro morphology, springback angle, microstructure and tensile properties of the alloy were studied and compared with those after traditional cold stamping. The results show that the hot forming with synchronous cooling process can be applied to forming 7075 aluminum alloy. The springback angle of the formed specimen was 0.03°, which was far lower than that after cold stamping. And the formed specimen had no buckling deformation. The microstructure of the formed specimen by hot forming with synchronous cooling was the same as that by the traditional cold stamping followed by solid solution treatment. After aging at 120℃ for 24 h, the yield strength and tensile strength were 553.98 MPa and 635.08 MPa, respectively, meeting the performance requirements of 7075 aluminum alloy in T6 temper qualified by the relevant standard.
  • WANG Rong, GAO Hao, WEI Deqiang
    Materials For Mechanical Engineering. 2017, 41(6): 34-38. https://doi.org/10.11973/jxgccl201706009
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    A medium carbon alloy steel was heat-treated by the liquid quenching and isothermal quenching with temperature process. The effects of austenitizing temperature and time, taking-out-of-liquid temperature and isothermal temperature and time on the microstructure and properties of the steel were discussed and the process was optimized. The results show that under the experimental condition, the ideal process parameters were as follows:Austenitizing temperature of 840℃ and holding time of 60 min, taking-out-of-liquid temperature of 238℃, isothermal temperature of 300℃ and isothermal time of 60 min. With this process, the matrix microstructure of the tested steel was composed of lower bainite and martensite, the hardness was 50 HRC, impact toughness was 26 J ·cm-2 and abrasion loss was 18 mg.
  • WANG Chaojie, LU Xiaofeng, LI Gang, LIU Luwei, ZHU Xiaolei, TU Shantung
    Materials For Mechanical Engineering. 2017, 41(6): 39-43. https://doi.org/10.11973/jxgccl201706010
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    Using the porous Ti-51%Ni (atom fraction) alloy with the porosities of 43%-58% as the research object, the micromorphology, phase composition, phase transformation behavior, and the compression and recovery properties under different compressive loads of the alloy were investigated. And the deformation mechanism was analyzed. The results show that the pores in the tested alloy distributed homogeneously. The porosity had little influence on the phase composition and phase transformation behavior. Two deformation mechanisms, namely the linear superelasticity and the saw-tooth plateau, were found under different compressive loads. At the stage of linear superelasticity, the tested alloy had relatively high compressibility and high recovery rate while almost lost the recovery ability at the stage of saw-tooth plateau.
  • LUO Sheji, WEN Ninghua, HAN Lihong
    Materials For Mechanical Engineering. 2017, 41(6): 44-48. https://doi.org/10.11973/jxgccl201706011
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    Fatigue tests under different stress amplitude were conducted on S135 drill pipe steel in air and H2S environments, and the fatigue lives under different conditions were obtained. The fatigue life formulas of the drill pipe steel in different environments were obtained by a data regression analysis method, and the fatigue fracture mechanism was analyzed. The results show that the tested steel had an obvious characteristic of fatigue limit in the air environment. The fatigue lives of tested steel in the H2S environment were lower than those in the air under the same equivalent stress amplitude, the fracture happened under relatively low equivalent stress amplitude and no fatigue limit existed. The fatigue cracks in the tested steel were all initiated at or near the surface in different environments and under different equivalent stress amplitude, and the crack initiation region exhibited mainly cleavage fracture. The crack propagation region showed a main characteristic of fatigue striations in the air while of cleavage fracture and cleavage steps in the H2S environment. On the cleavage fracture surface existed lots of second cracks, indicating a characteristic of hydrogen embrittlement fracture.
  • FAN Zhao, XU Wei, CHEN Weimin, WANG Guanghui
    Materials For Mechanical Engineering. 2017, 41(6): 49-54. https://doi.org/10.11973/jxgccl201706012
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    The microstructure and mechanical properties of HP40Nb steel furnace tube in a hydrogen reformer after 15-year service were studied by optical microscope, scanning electron microscope, energy dispersive spectrometer, tensile and impact testers. Based on the high-temperature creep rupture testing results, the remnant life of the furnace tube was evaluated. The results show that after the long-term high-temperature service, in the microstructure of furnace tube steel, the grain boundaries coarsened with the G phase precipitation; secondary carbides precipitated in grains obviously; creep voids were observed near inner and outer wall and in matrix; oxidation and chromium depletion were observed near inner and outer wall; decarburization layer was formed on the outer wall. Compared with the as-cast steel furnace tube, the tensile strength of the furnace tube after the long-term high-temperature service reduced by 30% and 18% at room and high temperature, respectively, the impact energy at room temperature decreased significantly, and the remnant life was less than 1 a.
  • WANG Lei, PAN Qirui, ZHU Song, WU Shezhang
    Materials For Mechanical Engineering. 2017, 41(6): 55-58. https://doi.org/10.11973/jxgccl201706013
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    Through the optimization design of material formula, friction blocks of copper-based powder metallurgy brake pad for high-speed train was prepared by the powder metallurgy method, and the physical and mechanical properties were tested. Then a new type of floating brake pad was assembled through the optimization of the pad structure, and the friction and wear properties of the pad were measured. The results show that shear strength of friction blocks for the brake pad was above 7 MPa. The average friction coefficients of the brake pad was 0.37±0.05 and the average wear loss was 0.126×10-6 cm3 ·J-1,which met the requirements of the friction and wear properties for brake pad specified by International Railway Union. The braking properties of the tested brake pad also met the requirements of the 350 km ·h-1 and above high-speed trains.
  • ZHANG Xiumei, PENG Kaiping
    Materials For Mechanical Engineering. 2017, 41(6): 59-62. https://doi.org/10.11973/jxgccl201706014
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    The 2-pass and 10-pass constrained groove pressing deformation were conducted on Q235 steel, respectively, and then the steel was annealed at different temperatures; the thermal stability of the groove pressed steel was studied. The results show that after annealing under 500℃, the microstructures of 2-pass and 10-pass groove pressed specimens were in the recovery stage. The grains were still uniform and fine equiaxed grains, similar to those before annealing. After annealing at 500-680℃, the recrystallization occurred in the specimens and the grains grew with the increase of annealing temperature. After annealing at 680℃, the microstructure of 10-pass groove pressed specimen was more uniform than that of 2-pass groove pressed specimen. With the increase of annealing temperature, the hardness of the 2-pass and 10-pass groove pressed specimens both decreased and the hardness decrease rate of 10-pass groove pressed specimen was relatively large after annealing at 250-600℃. However, the hardness was slightly higher than that of 2-pass groove pressed specimen after annealing at 680℃.
  • ZHANG Jinkai, CHENG Mengqi, WEI Xingqiao, WU Laizhi, WANG Liqiang, LÜ Weijie
    Materials For Mechanical Engineering. 2017, 41(6): 63-68. https://doi.org/10.11973/jxgccl201706015
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    Friction stir processing was utilized to prepare silver-loaded layer on the surface of Ti-6Al-4V (TC4) titanium alloy successfully. The morphology, distribution and influence on the mechanical properties of silver in the silver-loaded layer were studied. The results show that a silver-loaded layer of 700 μm in thickness was successfully fabricated. A large number of silver nanocrystallines with 10 nm in average diameter were observed in the top surface of silver-loaded layer due to mechanical nanocrystallization resulted from strong stirring shear force. In the sub-surface of silver-loaded layer, silver particles precipitated and formed a solid bonding with the matrix and free particles would barely appear in service. Uniformly distributed silver particles made the surface nanohardness of the silver-loaded layer about 30% higher than that of the silver-free zone, while it had little effect on the elastic modulus of the matrix.
  • CHEN Haipeng, WANG Fazhan
    Materials For Mechanical Engineering. 2017, 41(6): 69-74. https://doi.org/10.11973/jxgccl201706016
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    The process of hot isostatic pressing (HIP) on tungsten copper alloy powder sealed in wrap was simulated by using DEFORM-2D finite element software, and densification law of blank was analyzed; orthogonal optimization schemes of temperature, pressure and time were established by cross-over test way and the contour line cloud figure of relative density in temperature and pressure plane was drawn. The best program parameters were also proposed. According to the results of simulation, hot isostatic pressing experiment was carried out. The results show that the densification firstly appeared in the blank's edge, and then appeared in its center. The best parameter scheme for HIP was 950℃/110 MPa/2 h, which made overall relative density of the blank be more than 96%. Under the best scheme, the maximum error between simulated and experimental results of relative density was 1.26%, and the average error was 0.2%.
  • WANG Min, ZHANG Chun, XIAO Haifeng, LI Bing, XI Jiansheng
    Materials For Mechanical Engineering. 2017, 41(6): 75-78. https://doi.org/10.11973/jxgccl201706017
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    Taking the typical feature structure, namely U-shaped beam, of automotive hot-stamped parts as the object, the high-temperature fracture phenomena of BR1500HS steel sheet during hot forming was predicted by the combination of high-temperature fracture criterion and numerical simulation. The effects of female die fillet radius R on the steel sheet fracture behavior were analyzed. The results show that the fracture locations predicted by the hot forming fracture prediction model of high strength steel agreed well with the experimental results, and the relative error was below 10% between the predicted and experimental punch temperatures, indicating the relatively high reliability of the model. With R increasing, the fracture initiation time of the plank increased. The fracture initiation located at the side wall of one end of the U-shaped beam, but these locations along the height direction were different. The plank fractured along the longitudinal direction of the U-shaped beam, and the secondary fracture occurred at the side wall of another end of the U-shaped beam when R was equal to 2 mm and 6.5 mm. The fracture tended to appear at the side wall of U-shaped beam near the mould corner with a relatively small corner radius.
  • WEN Lianghua, LI Xiaotao, LI Xu, CAO Shihao, JIANG Xiaoyu
    Materials For Mechanical Engineering. 2017, 41(6): 79-83. https://doi.org/10.11973/jxgccl201706018
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    Using the finite element software ANSYS and combining the fatigue and wear coupling model, the equivalent stress intensity factors of cracks were simulated and calculated when the 10-ton wheel rolled over on the rail surface crack that had an initial length of 100 μm and an extension angle of 30°. The relationship between rail fatigue and wear was investigated and the propagation directions of the main and secondary cracks and the propagation behavior of main cracks after the secondary cracks appearing were also analyzed. The results show that the destruction mode of the rail gave priority to fatigue damage. When the branched cracks appeared, the stress concentration at the main crack tip would be relatively largely relieved, resulting in a relatively rapid decrease of the equivalent stress intensity factor. After the crack propagation length reached over 1 mm, the main crack further propagation process was accompanied by the appearance of secondary cracks; the propagation direction of the main crack remained unchanged and the propagation rate increased gradually, while the propagation directions and rates of the secondary cracks remained unchanged.
  • HUANG Yuanchun, WANG Sanxing, XIAO Zhengbing, LI Wenjing, HUANG Yutian, LIU Hui
    Materials For Mechanical Engineering. 2017, 41(6): 84-89. https://doi.org/10.11973/jxgccl201706019
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    The compression deformation experiments with the deformation amount of 60% were conducted on 35CrMo steel ingot blank at deformation temperatures of 850-1 150℃ and strain rates of 0.01-50 s-1 by using Gleeble-3810 thermal simulator. Combining with the characteristics of true stress-true strain curves, the influence of strain rate and deformation temperature on the microstructure of the steel was investigated. The results show that the microstructures of the tested steel all had dynamic recrystallization characteristics after compression deformation under different conditions. At the same strain rate, the dynamic recrystallization grains after compression became larger in size with the deformation temperature increasing; at the same deformation temperature, the dynamic recrystallization grains became smaller in size with the increase of the strain rate. After hot compression deformation, the grain size at different spots of the tested steel was different. The grains in the large deformation zone at the central area is the smallest in size, and with the increase of the vertical distance and the horizontal distance from the central area, the grain size gradually increased.
  • LIU Guohui, CHE Hongyan, MA Lei, YU Siliang, CAO Rui
    Materials For Mechanical Engineering. 2017, 41(6): 90-94. https://doi.org/10.11973/jxgccl201706020
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    The numerical simulation of stress distribution in aluminum-steel dissimilar metal welded joint during cold metal transition (CMT) welding was carried out by using ABAQUS finite element software. The variation law of stress distribution was analyzed and verified by experiments. The results show that at different welding times, the von Mises stresses unsymmetrically distributed at steel plate side and Al alloy plate side in the welded joint. And the stresses at Al alloy plate side were smaller than those at steel plate side. During the welding process, the longitudinal stress near the weld changed from the compressive stress into tensile stress, while the lateral stress at the welding initiating stage was tensile stress, then changed into compressive stress and then tensile stress. The longitudinal residual tensile stresses reached the largest values in the heat affect zone near the side of steel plate and Al alloy plate, which were 125 MPa and 208 MPa, respectively, while the peak values of lateral residual compressive stress were almost the same at both sides, which was about 80 MPa. The goodness-of-fit between the simulated and test results of residue stress distribution was 0.75, indicating the accuracy of the simulation results.
  • ZHANG Benguo, ZHAO Jian, XIA Jiansheng, FAN Lifeng
    Materials For Mechanical Engineering. 2017, 41(6): 95-98. https://doi.org/10.11973/jxgccl201706021
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    The reason for fracture of high-strength 35CrMo steel bolt during necking process was analyzed by the methods such as chemical composition analysis, microstructure and fracture observation and mechanical property testing. The results show that the fracture of 35CrMo steel bolt had a typical brittle fracture characteristic. The microstructue of the 35CrMo steel was non-uniform, resulting in the relatively low tensile strength. During the straightening of necking process, when the pulling force at the necking part of the bolt was relatively high, the bolt fractured.
  • LIN Yang
    Materials For Mechanical Engineering. 2017, 41(6): 99-102. https://doi.org/10.11973/jxgccl201706022
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    Using the test methods of macroscopic observation, metallographic examination, electronic microscope and energy spectrum analysis, the perforation failure cause at the elbow of crude oil terminal pipeline was analyzed. The results show that the inner-wall at outer arc side of the elbow pipe was eroded by the oil and gas medium in the pipeline, leading to the decrease of the pipe wall thickness, which caused the perforation failure; the decrease of outer-wall thickness at outer arc side of the elbow pipe caused by corrosion also had some effects on the failure. In order to prevent the perforation failure, the weld reinforcement of the straight and elbow pipes join should be controlled carefully during the welding of pipeline, realizing the reduction of turbulence to reduce the erosion of elbow pipe. Also the external protection of the pipelines should be considered.