20 June 2019, Volume 43 Issue 6
    

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  • HU Li, ZHANG Guikai, TANG Tao
    Materials For Mechanical Engineering. 2019, 43(6): 1-7. https://doi.org/10.11973/jxgccl201906001
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    Preparation of FeAl/Al2O3 tritium permeation barrier consisting of FeAl alloy transition layer and Al2O3 film on the layer's surface by substrate aluminization and subsequent selective oxidation is now the first choice of tritium permeation barrier technology. The Al2O3 film plays a key role on the service performance of FeAl/Al2O3 tritium permeation barrier. Surface oxidation behaviors of the FeAl alloy and coating, including selective oxidation of Al, oxidation thermodynamic and kinetic behavior and oxidation mechanism, are reviewed. Influence of substrate elements on Al2O3 film forming as well as its structure and the low temperature preparation technology of Al2O3 film on surface of the tritium permeation barrier are discribed. The future research direction of FeAl/Al2O3 tritium permeation barrier is proposed.
  • NIE Xiaoqian, ZHANG Chengcheng, WANG Runzi, ZHANG Xiancheng, TU Shantong
    Materials For Mechanical Engineering. 2019, 43(6): 8-11,17. https://doi.org/10.11973/jxgccl201906002
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    Fatigue test without load-holding and creep-fatigue tests with load-holding at maximum tension/compression strains were conducted on domestic powder metallurgy nickel-based superalloy FGH96 under total strain control at 650℃. The failure life and failure mode of the alloy were studied, and the failure life was compared with that of as-cast nickel-based superalloy GH4169. The results show that the introduced load-holding process reduced the failure life of the FGH96 superalloy. Compared with load-holding at maximum tension strain, the creep damage produced during load-holding at the maximum compression strain was larger, resulting in a shorter failure life. The fatigue failure lives of FGH96 superalloy were higher than those of GH4169 superalloy, and the creep-fatigue failure lives were lower than those of GH4169 superalloy at relatively high strain amplitude (larger than 1.4%), while the opposite was true at relatively low strain amplitude (lower than 1.4%). The fatigue fracture and creep-fatigue fracture of FGH96 superalloy both showed mutiple crack initiation failure characteristics on surface or near surface.
  • ZHOU Shuang, TAN Jianping, LIU Changjun, ZHANG Haoyu, CHEN Jin
    Materials For Mechanical Engineering. 2019, 43(6): 12-17. https://doi.org/10.11973/jxgccl201906003
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    Coarse-grained heat-affected zone (CGHAZ) simulation specimens of 2.25Cr1Mo0.25V steel welded joint were prepared with different parameters, and the optimal thermal simulation parameters were determined by comparing hardness, grain size and microstructure with those of the actual joint CGHAZ. And then the CGHAZ specimen was simulated with the optimal parameters. The stress relaxation behavior of the specimen at 675℃ was studied, the reheat cracking process was analyzed, and the reheat cracking strain criterion was obtained. The results show that the optimal thermal simulation parameters were listed as follows:heat input of 30 kJ·cm-1, preheating temperature of 200℃, heating rate of 1 000℃·s-1, peak temperature of 1 320℃, time on peak temperature of 1 s. The microstructure of the obtained CGHAZ specimen consisted of lath bainite, with grain size of grade 4.5. The stress relaxation behaviors of CGHAZ specimen were similar under different initial stresses. The critical failure creep strains were all about 0.31%. The critical failure creep strain can be regarded as the reheat cracking strain criterion, and can be used to evaluate the post-welding heat treatment process of the steel as the creep strain demarcation point for characterizing the sensitivity of CGHAZ reheat crack.
  • ZHANG Wei, WANG Xiaowei, GONG Jianming, LI Xiang, ZHANG Tianyu
    Materials For Mechanical Engineering. 2019, 43(6): 18-22. https://doi.org/10.11973/jxgccl201906004
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    Cyclic loading tests at 650℃ for different number of cycles were conducted on P92 steel, and then tensile tests at 650℃ were carried out on the steel. The effects of cyclic deformation on microstructure and high temperature tensile property were studied. The results show that the microstructure of P92 steel without cyclic deformation consisted of fine lath martensite; subgrains and dislocations existed inside the martensite and M23C6 carbide precipitated on the boundaries. After cyclic deformation, the recovery of the lath martensite in the steel occurred obviously, the subgrains grew and the dislocations changed to the cellular-like structure. Compared with those without cyclic deformation, the high temperature tensile properties of the P92 steel after cyclic deformation decreased significantly, and the tensile strength and yield strength decreased with the increase of the number of cycles. The cyclic deformation did not greatly influence the tensile fracture mechanism of the P92 steel; dimples appeared on the tensile fracture surface, indicating that the tensile fracture mechanism was ductile fracture.
  • YAN Ruifeng, CHEN Sijie, DING Guangzhu, WANG Qitao
    Materials For Mechanical Engineering. 2019, 43(6): 23-27. https://doi.org/10.11973/jxgccl201906005
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    T91 steel was welded by simulated three-temperature process of transient liquid phase diffusion welding, and then tempered at 780℃ for 2 h. The microstructure and mechanical properties of the heat-affected zone and the effect of tempering treatment on the mechanical properties of the heat-affected zone were studied. The results show that the heat-affected zone was divided into four zones:overheated coarse lath martensite zone at 0-7.5 mm distance from the weld, fine lath martensite zone at 7.5-22.5 mm distance from the weld, ferrite+martensite zone at 22.5-37.5 mm distance from the weld and tempered martensite zone at 37.5-42.5 mm distance from the weld. With increasing distance from the weld, the hard and brittle tendency of the heat-affected zone decreased and the fracture mechanism changed from brittle fracture to ductile fracture. Compared with those before tempering, the tensile strength and hardness of the heat-affected zone after tempering decreased but the toughness increased.
  • HAN Hongguang, SHEN Junjie, XIE Jiaxing
    Materials For Mechanical Engineering. 2019, 43(6): 28-32. https://doi.org/10.11973/jxgccl201906006
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    P92 heat-resistant steel was aged at 650℃ for 600, 1 200 h, respectively, and then subjected to uniaxial tensile creep test at 170 MPa and 650℃. The microstructures of the tested steel after aging and creep rupture were observed and the creep-rupture property was analyzed. The results show that after aging, the lath martensite in the tested steel was coarsened, and Laves phase precipitated in the structure. The longer the aging time, the larger the number and the diameter of the Laves phase. After creep rupture, the lath martensite in the structure near fracture became equiaxed. After aging, the creep rupture life of the tested steel was shortened but the creep rupture strain increased, indicating the decrease in the creep-rupture property. The tested steel before and after aging both fractured in ductile during creep, and the dimples on the creep rupture fracture after aging were relatively small and relatively shallow.
  • LU Chao, LIANG Hao, ZHANG Bingjie, SUN Wenwei, ZHANG Zhihui, ZHOU Xiaomeng, MAO Xiangyang
    Materials For Mechanical Engineering. 2019, 43(6): 33-37,42. https://doi.org/10.11973/jxgccl201906007
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    Ultrasonic impact treatment was conducted on as-cast semi-high speed steel with surface presetting chrome powder, and then the steel was annealed at 450℃ for 2 h. The microstructure and high-temperature (450℃) wear resistance of the surface layer before and after treatment were studied. The results show that the as-cast structure of the tested steel consisted of sorbite and carbides. After ultrasonic impact and annealing treatment, the cemetite lamellae in sorbite was broken and spherized, and the structure of the surface layer was refined. After ultrasonic impact and annealing treatment, the surface hardness of the tested steel increased, the hardness in the surface layer distributed in gradient, and the thickness of the hardening layer reached 2.5 mm. Moreover, the high-temperature wear resistance was improved; the wear rate decreased from the as-cast 0.997 mg·min-1 to 0.640 mg·min-1, the friction coefficient decreased from the as-cast 0.547 to 0.509, and the abrasive wear degree also decreased.
  • ZHENG Wenbin, CHEN Hansheng, WANG Huanping, GAO Ren, ZHU Qingong, YANG Qinghua, XU Shiqing, ZHANG Xianghua
    Materials For Mechanical Engineering. 2019, 43(6): 38-42. https://doi.org/10.11973/jxgccl201906008
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    SiO2-Al2O3-MgO glasses doped with 0-3.0wt% Li2O were prepared by conventional melt quenching technique, and the effects of Li2O doping amount on thermal property, structural stability and mechanical properties of the glass were investigated. The results show that the doping of Li2O reduced the softening temperature of the glass effectively. With the increase of Li2O doping amount, the optical band gap of the glass decreased first and then increased, while the structural stability, thermal stability and mechanical properties increased first and then decreased. When the Li2O doping amount was 1.0wt%, the glass had the most stable structure and the best bending and compressive properties.
  • YAN An, FANG Zhan, CHEN Ke, DONG Fengbo, GUO Lijie, ZHANG Lanting, SHAN Aidang
    Materials For Mechanical Engineering. 2019, 43(6): 43-49. https://doi.org/10.11973/jxgccl201906009
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    Two-millimeter thick 2195 Al-Li alloy plates were welded by friction stir welding at different welding speeds (100-300 mm·min-1). The effects of welding speed on tensile properties of the joint at room and cryogenic (-183℃) temperatures were studied. The difference in the change of tensile properties between the joint and base metal from room temperature to cryogenic temperature was also investigated. The results show that the yield strength and tensile strength of the joint at cryogenic temperature and different welding speeds were higher than those at room temperature. When the welding speed was 200 mm·min-1, the tensile properties of the joint at room and cryogenic temperatures were the best. From room temperature to cryogenic temperature, the increase ranges of the tensile strength and ductility of the joint were higher than those of the base metal, indicating that the increase degree in tensile properties of the joint at cryogenic temperature was larger than that of the base metal. With increasing welding speed, the tesile fracture positions shifted from the near retreating side spot in the weld nugget zone to the zigzag line.
  • LI Yuqin, XIAO Gang, LI Tao
    Materials For Mechanical Engineering. 2019, 43(6): 50-52. https://doi.org/10.11973/jxgccl201906010
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    Ultrasonic vibration assisted grinding and conventional grinding without ultrasonic vibration were conducted on GCr15 bearing steel, and then the grinding surface residual stresses were measured. The effects of ultrasonic vibration as well as grinding depth (5-30 μm) and linear speed of grinding wheel (2-12 m·s-1) on the surface residual stress were studied. The results show that the residual compressive stresses were generated on the surfaces grinded by the two methods. The surface residual compressive stress obtained by the ultrasonic vibration assisted grinding was relatively high. With increasing feed depth or decreasing linear speed of grinding wheel, the surface residual compressive stresses by the two methods both generally increased. With increasing linear speed of grinding wheel, the difference value between the surface residual compressive stresses with and without ultrasonic vibration was reduced, indicating that the improvement effect of the ultrasonic vibration on the surface residual compressive stress was weakened.
  • MA Xiaoming, ZHANG Yingying
    Materials For Mechanical Engineering. 2019, 43(6): 53-57,81. https://doi.org/10.11973/jxgccl201906011
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    A flow booster coupling bracket joint bolt fractured during operation. The reason for fracture of the bolt was investigated by fracture morphology observation, chemical composition analysis, hardness testing, microstructure analysis, intensity check and finite element simulation. The results show that the bolt failed in fatigue fracture. The stress concentration at the root of the first thread at the joint of the bolt and nut was obvious. Under the alternating tension loading, cracks initiated at the spot and propagated until the bolt fractured. The low content of nickel and molybdenum in the bolt material, the high hardness, the defects such as holes and inclusions in the structure, the obvious stress concentration at the root of the thread and the large alternating stress amplitude were the main factors leading to the fatigue fracture of the bolt.
  • HU Xiaobing, XIE Lili, HE Meng, ZHU Zhigang
    Materials For Mechanical Engineering. 2019, 43(6): 58-63,71. https://doi.org/10.11973/jxgccl201906012
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    Copper oxide (CuO) is a typical p-type semiconducting metal oxide. As a sensing material, pure CuO has more or less defects; therefore, a series of modification methods are applied to improve the gas sensitivity of CuO. Recent advances in gas sensors based on CuO and its composites are reviewed, and the existing problems of CuO-based gas sensors and future research direction are proposed.
  • CHEN Yu, HU Chi, XU Qian, XIE Shaoxiong, XU Jiageng, LONG Tao, WANG Qingyuan, SHI Wei, ZHU Jianguo
    Materials For Mechanical Engineering. 2019, 43(6): 64-71. https://doi.org/10.11973/jxgccl201906013
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    Domain structure is deemed as the remarkable microstructural feature of ferroelectric materials, and its spontaneous polarization vector can be switched by the external applied electric/mechanical field (namely domain switching), leading to multiply electromechanical properties of ferroelectric materials. Starting from the theory of domain switching, research progress on the domain switching criterion is reviewed, and research results of the domain-wall dynamics and the domain switching-dependent fracture mechanics are described. It is aimed at providing some references for the micromechanics research of ferroelectric materials.
  • YAO Xiaocheng, ZHAO Cheng, ZENG Tao
    Materials For Mechanical Engineering. 2019, 43(6): 72-76. https://doi.org/10.11973/jxgccl201906014
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    On the basis of active and passive vibration control principles, four piezoelectric smart materials used in vibration control field, including single layer piezoelectric ceramics, multi-stacked piezoelectric ceramics, piezoelectric fiber composite and 0-3 type piezoelectric composite, are reviewed. The research progress of the structural characteristics, preparation process of the materails and their application for vibration attenuation in the fields of machinery manufacturing, aerospace and marine shipping are highlighted. The research direction in future of the piezoelectric materials is proposed.
  • ZHANG Dong, DING Shihua
    Materials For Mechanical Engineering. 2019, 43(6): 77-81. https://doi.org/10.11973/jxgccl201906015
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    Bi1.5-xBaxZnNb1.5O7(x=0.05, 0.10, 0.15, 0.20, molar ratio) ceramics were prepared by solid sintering method. The effects of barium doping on sintering property, structure and dielectric property of the ceramics were studied. The results show that the sintering temperature of the ceramics decreased from 1 050℃ to 960℃ after barium doping. The phase of the ceramics was composed of single pyrochlorite, and its diffraction peak shifted to a small angular direction as the doping amount of barium increased. The dielectric constant and dielectric loss of the ceramics increased with increasing barium doping amount. Under different frequencies, the ceramics with different barium doping amount showed dielectric relaxation at low temperatures. The dielectric relaxation peak became widening and flattening with increasing barium doping amount, and shifted to high temperature directions. With increasing barium doping amount, the dielectric relaxation degree of the ceramics decreased first and then increased, and the relaxation activation energy and temperature coefficient increased first and then decreased.
  • YANG Sinuo, TANG Tiande, ZHOU Qin, ZHAO Cheng, XIONG Zhengwei
    Materials For Mechanical Engineering. 2019, 43(6): 82-85. https://doi.org/10.11973/jxgccl201906016
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    Sr2Nb2O7 powder was prepared by solid-state reaction method, and then Sr2Nb2O7 ceramics were prepared by two-step textured sintering process. The microstructure, phase composition and the change of resistivity with temperature and time of the ceramics were studied. The results show that the ceramics had a pure phase. The structure was composed of plate-like grains and the grains were oriented well along the pressing direction. The high temperature resistivity of the ceramics decreased with the increase of temperature. During holding at 800℃ for 125 h, the resistance of the perpendicular samples (normal direction of the sample surface was perpendicular to the pressing direction) did not deteriorate. At 980℃ and 1 000℃, the perpendicular samples showed resistance degradation behavior, and the breakdown occurred after holding for 20 h and 1 h, respectively. At 1 000℃, the parallel sample (normal direction of the sample surface was parallel to the pressing direction) had relatively long degradation time of resistivity because of the relatively large number of grain boundaries.